ÀèÆ¬¥Ú¡¼¥¸¤Ø ľÁ°¤Î¥Ú¡¼¥¸¤Ø ¼¡¤Î¥Ú¡¼¥¸¤Ø ºÇ½ª¥Ú¡¼¥¸¤Ø

Bile acid

LIPID_IDBA0103

CHEM_NA3¦Á,6¦Á,7¦Â-TRIHYDROXY-5¦Á-CHOLAN-24-OIC

ACID

COMMON_NAALLO ¦Ø-MURICHOLIC ACID

MOL_FORMULAC24H40O5

MOL_WT408

MELT_PT242-244¡¬C(from EtOAc),192-193¡¬C(Me ESTER)(172)

BOIL_PT

OPT_ROT

REFRA_IND

DENSITY

SOLUBILITY

UV_SPEC

IR_SPEC1685cm-1(C=O), 3481,1007cm-1(OH)(172)

NMR_SPEC1H-NMR(CDCl3+DMSO-d6) 0.67(s,18-Me),

0.79(s,19-Me), 0.93(d,J=6.3Hz,21-Me), 3.02(brm,6¦Â-

and 7¦Á-H),

4.00(m,3¦Â-H)C17=56.18,C18=12.25,C19=12.54,C20=

35.50,C21=18.47,C22=31.20,

C23=31.27,C24=175.56,CCOOMe=51.93

(172)13C-NMR(Me ESTER)(CDCl3+10% MeOH-d4)

C1=32.62,C2=28.66,C3=65.76,C4=30.06,

C5=42.10,C6=75.27,C7=80.64

MS_SPECMe ESTER M/Z(RELATIVE INTENSITY)

404(54%,M-H2O), 386(100%,M-2H2O),

368(48%,M-3H2O), 289(34%), 271(49%), 262(21%),

NOTE_SPEC

SOURCE

BIOL_ACTIV

NOTE

1998ǯ10·î26Æü103 / 591 ¥Ú¡¼¥¸