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Bile acid

LIPID_IDBA0105

CHEM_NA3¦Á,6¦Â,7¦Â,12¦Á-TETRAHYDROXY-5¦Á-CHOLAN-2

4-OIC ACID

COMMON_NA

MOL_FORMULAC24H40O6

MOL_WT424

MELT_PT235-237¡¬C(FROM EtOAc/HEXANE),151-152¡¬C(Me

ESTER)(172)

BOIL_PT

OPT_ROT

REFRA_IND

DENSITY

SOLUBILITY

UV_SPEC

IR_SPEC1698cm-1(C=O), 3525,1033,1014cm-1(OH)(172)

NMR_SPEC1H-NMR(CDCl3+20%

DMSO-d6)0.69(s,18-Me),0.93(s,19-Me),0.99(d,J=6.3H

z,21-Me),

3.25(brm,7¦Á-H),3.51(m,6¦Á-H),3.92(m,12¦Â-H),4.06(

m,3¦Â-H)(172) 13C-NMR(Me ESTER)

C1=32.95,C2=29.04,C3=66.45,C4=34.06,C5=40.38,C6

=75.02, C7=76.58,C8=38.23,C9=45.33,C

C17=47.13,C18=12.90,C19=14.81,C20=35.14,C21=17

.48,C22=31.00,

MS_SPECMe ESTER M/Z(RELATIVE INTENSITY)

420(2%,M-H2O), 402(16%,M-2H2O),

384(10%,M-3H2O), 305(100%), 287(57%), 269(91%),

NOTE_SPEC

SOURCE

BIOL_ACTIV

NOTE

1998ǯ10·î26Æü105 / 591 ¥Ú¡¼¥¸